摘要：A two-dimensional solid of KSbMoO5 has been synthesized by hydrothermal methods and structurally characterized by X-ray crystallography. It crystallizes in the monoclinic system, space group P21/c with a = 9.2084(7), b = 11.3155(7), c = 5.6691(3) (A), β = 107.624(3)°, V = 562.98(6) (A)3, Z = 4, Mr = 336.79, Dc = 3.974 g/cm3, F(000) = 608 and ((MoKα = 7.697 mm-1. The final R = 0.0496 and wR = 0.1294 for 888 observed reflections with I > 2σ(Ⅰ). The structure is built up of SbMoO5-layers, between every two of which sodium cations are located.

关键词：热液合成 晶体结构 ksbmoo5 x射线衍射分析 钼 

单位：DepartmentofChemistry; FuzhouUniversity; Fuzhou350002; China／／StateKeyLaboratoryofStructuralChemistry; Fuzhou350002; China; DepartmentofChemistry; FuzhouUniversity; Fuzhou350002; China